(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

Base Information

Chemical Name:(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine
CAS No.:157794-61-1
Molecular Formula:C₂₆H₂₅NO₄
Molecular Weight:415.489
Hs Code.:

Synonyms:(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

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Chemical Property of (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

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Technology Process of (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

There total 1 articles about (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 152774-49-7
2-amino-2-benzylbut-3-enoic acid

: 501-53-1,94274-21-2
benzyl chloroformate

: 157794-61-1
(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

Guidance literature:: With dmap; triethylamine; In dimethyl sulfoxide; at 50 ℃; for 1.5h;
DOI:10.1021/jo00097a064

Reference yield: 61.0%

: 157794-61-1
(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

: (2S,3S)-2-Benzyl-2-benzyloxycarbonylamino-3,4-dihydroxy-butyric acid benzyl ester

: (2S,3R)-2-Benzyl-2-benzyloxycarbonylamino-3,4-dihydroxy-butyric acid benzyl ester

Guidance literature:: With osmium(VIII) oxide; N-methyl-2-indolinone;
DOI:10.1021/jo00122a002

Reference yield:

: 157794-61-1
(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylphenylalanine

: (S)-2-Amino-2-(S)-oxiranyl-3-phenyl-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / OsO₄, NMO

2: 81 percent / pyridine

3: 72 percent / LDA / tetrahydrofuran

4: H₂ / Pd(OH)2/C

With pyridine; osmium(VIII) oxide; N-methyl-2-indolinone; hydrogen; lithium diisopropyl amide; palladium dihydroxide; In tetrahydrofuran;
DOI:10.1021/jo00122a002