p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Base Information

Chemical Name:p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside
CAS No.:218617-29-9
Molecular Formula:C₂₇H₃₉NO₁₇
Molecular Weight:649.603
Hs Code.:

Synonyms:p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

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Chemical Property of p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

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Technology Process of p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

There total 14 articles about p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 814-68-6,25189-84-8
acryloyl chloride

: 467219-65-4
p-aminophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

: 218617-29-9
p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Guidance literature:: With triethylamine; In methanol; at 0 - 20 ℃; for 2h;
DOI:10.1016/S0040-4039(98)01897-8

Reference yield:

: 148705-02-6
p-nitrophenyl 2,3,6,2',6'-penta-O-acetyl-β-lactoside

: 218617-29-9
p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 38 percent / 4 Angstroem MS; AgClO₄; SnCl₂ / CH₂Cl₂ / 12 h / 0 °C

2: 97 percent / NaOMe / methanol / 6 h / 20 °C

3: 29 mg / 10 N HCl / 10 percent Pd(OH)2 / methanol / 6 h / 20 °C

4: 93 percent / Et₃N / methanol; CHCl₃ / 1.5 h / 20 °C

With hydrogenchloride; 4 Angstroem MS; sodium methylate; silver perchlorate; triethylamine; tin(ll) chloride; palladium dihydroxide; In methanol; dichloromethane; chloroform;
DOI:10.1016/S0008-6215(02)00093-9

Reference yield:

: 218617-05-1
p-nitrophenyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1->3)-2,6-di-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 218617-29-9
p-N-acryloylamidophenyl (α-D-galacopyranosyl)-(1->3)-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaOMe / methanol / 6 h / 20 °C

2: 29 mg / 10 N HCl / 10 percent Pd(OH)2 / methanol / 6 h / 20 °C

3: 93 percent / Et₃N / methanol; CHCl₃ / 1.5 h / 20 °C

With hydrogenchloride; sodium methylate; triethylamine; palladium dihydroxide; In methanol; chloroform;
DOI:10.1016/S0008-6215(02)00093-9