C₄₅H₆₃N₃O₈

Base Information

Chemical Name:C₄₅H₆₃N₃O₈
CAS No.:1026961-63-6
Molecular Formula:C₄₅H₆₃N₃O₈
Molecular Weight:774.011
Hs Code.:

C<sub>45</sub>H<sub>63</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₄₅H₆₃N₃O₈

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Chemical Property of C₄₅H₆₃N₃O₈

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Technology Process of C₄₅H₆₃N₃O₈

There total 16 articles about C₄₅H₆₃N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 945496-83-3
C₄₆H₆₅N₃O₈

: 1026961-63-6
C₄₅H₆₃N₃O₈

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1039/b703116e

Reference yield:

: C₂₁H₂₄N₂O₅

: 1026961-63-6
C₄₅H₆₃N₃O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: TFA / CH₂Cl₂ / 1 h / 20 °C

1.2: 4.50 g / benzaldehyde / ethyl acetate / 0 - 20 °C

2.1: hydroxylamine hydrochloride / methanol / 0.33 h / 60 °C

3.1: SOCl₂ / 16 h / 0 - 20 °C

4.1: 2.89 g / NaHCO₃ / CH₂Cl₂ / 16 h / 20 °C

5.1: DIPEA / methanol

6.1: 100 percent / H₂ / Pd-C / methanol / 0.75 h / 20 °C

7.1: 0.425 g / EDC; HOAt; DMAP / dimethylformamide / 16 h / 20 °C

8.1: 100 percent / LiOH / tetrahydrofuran; H₂O / 12 h / 20 °C

With dmap; lithium hydroxide; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/b703116e

Reference yield:

: 440679-63-0,945496-80-0
C₂₁H₂₄N₂O₅

: 1026961-63-6
C₄₅H₆₃N₃O₈

Guidance literature:: Multi-step reaction with 7 steps

1: hydroxylamine hydrochloride / methanol / 0.33 h / 60 °C

2: SOCl₂ / 16 h / 0 - 20 °C

3: 2.89 g / NaHCO₃ / CH₂Cl₂ / 16 h / 20 °C

4: DIPEA / methanol

5: 100 percent / H₂ / Pd-C / methanol / 0.75 h / 20 °C

6: 0.425 g / EDC; HOAt; DMAP / dimethylformamide / 16 h / 20 °C

7: 100 percent / LiOH / tetrahydrofuran; H₂O / 12 h / 20 °C

With dmap; lithium hydroxide; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/b703116e