((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃BN₂H₂C₁₀H₆

Base Information

• Chemical Name: ((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃BN₂H₂C₁₀H₆
• CAS No.: 1159803-41-4
• Molecular Formula: C₇₆H₈₅BN₂O₄
• Molecular Weight: 1101.33
• Mol file: 1159803-41-4.mol

Synonyms:((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃BN₂H₂C₁₀H₆

Chemical Property of ((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃BN₂H₂C₁₀H₆

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃BN₂H₂C₁₀H₆

There total 1 articles about ((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃BN₂H₂C₁₀H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

5-1,8-naphthalenediaminatoborane-1,3-dibromobenzene (1098071-09-0) + (C6H13OC6H4)2C6H3B(OH)2 (1204226-81-2) → ((C6H13OC6H4)2C6H3)2C6H3BN2H2C10H6 (1159803-41-4)

Guidance literature:

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In tetrahydrofuran; water; at 80 ℃; for 24h;

DOI:10.1016/j.jorganchem.2008.11.068

Reference yield:

((C6H13OC6H4)2C6H3)2C6H3BN2H2C10H6 (1159803-41-4) → ((C6H13OC6H4)2C6H3)2C6H3B(OH)2 (1204226-82-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water;

DOI:10.1016/j.jorganchem.2008.11.068

Reference yield:

((C6H13OC6H4)2C6H3)2C6H3BN2H2C10H6 (1159803-41-4) + water (7732-18-5) → ((C6H13OC6H4)2C6H3)2C6H3B(OH)2 (1204226-82-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; aq. HCl added to a soln. at room temp., stirred at room temp. for 8 h; aq. HCl added, filtered (Celite), extd. (diethyl ether), dried (MgSO4), evapd. (vac.); NMR;

DOI:10.1016/j.jorganchem.2008.11.068

upstream raw materials:

5-1,8-naphthalenediaminatoborane-1,3-dibromobenzene

(C₆H₁₃OC₆H₄)2C₆H₃B(OH)2

Downstream raw materials:

((C₆H₁₃OC₆H₄)2C₆H₃)2C₆H₃B(OH)2