3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

Base Information

Chemical Name:3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide
CAS No.:107356-07-0
Molecular Formula:C₁₈H₂₁Cl₂N₃O₅
Molecular Weight:430.288
Hs Code.:

Synonyms:3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

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Chemical Property of 3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

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Technology Process of 3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

There total 6 articles about 3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98033-85-3
5-(5-bromopentyl)-3-methylisoxazole

: 107356-07-0
3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / Amberlyst A-26 (carbonate form) / benzene / 4 h / Heating

2: 78 percent / triphenylphosphine, diethyl azodicarboxylate / CH₂Cl₂ / Ambient temperature

3: 95 percent / LiOH / methanol; H₂O / 18 h / Heating

4: SOCl₂ / 16 h / Ambient temperature

5: Et₃N / CHCl₃ / 16 h / Ambient temperature

With lithium hydroxide; thionyl chloride; Amberlyst A-26 (carbonate form); triethylamine; triphenylphosphine; diethylazodicarboxylate; In methanol; dichloromethane; chloroform; water; benzene;
DOI:10.1021/jm00122a027

Reference yield:

: 118276-21-4
3-Methyl-5-(5-hydroxypentyl)isoxazole

: 107356-07-0
3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / triphenylphosphine, diethyl azodicarboxylate / CH₂Cl₂ / Ambient temperature

2: 95 percent / LiOH / methanol; H₂O / 18 h / Heating

3: SOCl₂ / 16 h / Ambient temperature

4: Et₃N / CHCl₃ / 16 h / Ambient temperature

With lithium hydroxide; thionyl chloride; triethylamine; triphenylphosphine; diethylazodicarboxylate; In methanol; dichloromethane; chloroform; water;
DOI:10.1021/jm00122a027

Reference yield:

: 118276-05-4
3-Chloro-4-<<5-(3-methyl-5-isoxazolyl)pentyl>oxy>-5-nitrobenzoic acid

: 107356-07-0
3-Chloro-N-(2-chloroethyl)-4-{[5-(3-methyl-5-isoxazolyl)pentyl]oxy}-5-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 16 h / Ambient temperature

2: Et₃N / CHCl₃ / 16 h / Ambient temperature

With thionyl chloride; triethylamine; In chloroform;
DOI:10.1021/jm00122a027