N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester

Base Information

Chemical Name:N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester
CAS No.:78817-99-9
Molecular Formula:C₄₅H₅₃N₅O₉
Molecular Weight:807.944
Hs Code.:

Synonyms:N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester

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Chemical Property of N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester

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Technology Process of N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester

There total 2 articles about N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 76698-53-8
glycyl-L-phenylalanyl-L-leucine methyl ester trifluoroacetate

: N-benzyloxycarbonyl-O-benzyltyrosylsarcosine

: 78817-99-9
N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 1 h; 2.) r.t., 24 h;

Reference yield:

: 52773-66-7
benzyloxycarbonyl-O-benzyl-L-tyrosine 1-succinimidyl ester

: 78817-99-9
N-benzyloxycarbonyl-O-benzyltyrosylsarcosylglycylphenylalanylleucylmethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 2N sodium hydroxide, sodium hydrogen carbonate / H₂O; dimethylformamide / 6 h

2: 86 percent / 1.) 1-hydroxybenzotriazole monohydrate, N,N'-dicyclohexylcarbodiimide, triethylamine / dimethylformamide / 1.) 0 deg C, 1 h; 2.) r.t., 24 h

With sodium hydroxide; sodium hydrogencarbonate; 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In water; N,N-dimethyl-formamide;