2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester

Base Information

Chemical Name:2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester
CAS No.:159395-36-5
Molecular Formula:C₂₄H₃₇N₂O₁₀P
Molecular Weight:544.539
Hs Code.:

2-<(S)-N-<Methoxy((S)-3'-(N-(benzyloxycarbonyl)amino)-4'-carbethoxybutyl)phosphinyl>amino>pentane-1,5-dioic acid diethyl ester

Synonyms:2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester

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Chemical Property of 2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester

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Technology Process of 2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester

There total 2 articles about 2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1118-89-4
diethyl-L-glutamate hydrochloride

: 159395-35-4
Methyl ((S)-3-(N-(benzyloxycarbonyl)amino)-4-carbethoxybutyl)phosphonochloridate

: 159395-36-5
2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00104a017

Reference yield:

: Methyl ((S)-3-(N-(benzyloxycarbonyl)amino)-4-carbethoxybutyl)phosphonic acid

: 159395-36-5
2-<(S)-N-amino>pentane-1,5-dioic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2, DMF / CH₂Cl₂ / 1.) 0 deg C, 20 min, 2.) r.t., 1.5 h

2: 64 percent / Et₃N / tetrahydrofuran

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00104a017