C₂₂H₂₉N₅

Base Information

Chemical Name:C₂₂H₂₉N₅
CAS No.:1304723-53-2
Molecular Formula:C₂₂H₂₉N₅
Molecular Weight:363.506
Hs Code.:

C<sub>22</sub>H<sub>29</sub>N<sub>5</sub>

Synonyms:C₂₂H₂₉N₅

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Chemical Property of C₂₂H₂₉N₅

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Technology Process of C₂₂H₂₉N₅

There total 9 articles about C₂₂H₂₉N₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1304723-52-1
C₃₅H₃₇N₅

: 1304723-53-2
C₂₂H₂₉N₅

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; at 20 ℃; for 16h;
DOI:10.1016/j.bmcl.2011.02.098

Reference yield:

: 1304723-50-9
(S)-7-benzyl-2,7-diazaspiro[4.5]decane

: 1304723-53-2
C₂₂H₂₉N₅

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 1 h / 80 °C

2: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / 7 h / 95 °C

3: hydroxylamine hydrochloride; sodium acetate / methanol / 16 h / 20 °C

With hydroxylamine hydrochloride; sodium acetate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; In 1-methyl-pyrrolidin-2-one; methanol; 2: Buchwald coupling;
DOI:10.1016/j.bmcl.2011.02.098

Reference yield:

: 1304723-51-0
C₂₂H₂₇ClN₄

: 1304723-53-2
C₂₂H₂₉N₅

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / 7 h / 95 °C

2: hydroxylamine hydrochloride; sodium acetate / methanol / 16 h / 20 °C

With hydroxylamine hydrochloride; sodium acetate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In methanol; 1: Buchwald coupling;
DOI:10.1016/j.bmcl.2011.02.098