1-Benzyl-1-methyl-1,4-dihydronaphthaline

Base Information

Chemical Name:1-Benzyl-1-methyl-1,4-dihydronaphthaline
CAS No.:147779-74-6
Molecular Formula:C₁₈H₁₈
Molecular Weight:234.341
Hs Code.:

Synonyms:1-Benzyl-1-methyl-1,4-dihydronaphthaline

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Chemical Property of 1-Benzyl-1-methyl-1,4-dihydronaphthaline

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Technology Process of 1-Benzyl-1-methyl-1,4-dihydronaphthaline

There total 4 articles about 1-Benzyl-1-methyl-1,4-dihydronaphthaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 147779-73-5
1-Benzyl-1-methyl-1,4-dihydronaphthalen-2-one p-toluenesulfonylhydrazone

: 147779-74-6
1-Benzyl-1-methyl-1,4-dihydronaphthaline

Guidance literature:: With methyllithium; In diethyl ether; at 0 ℃; for 1.5h;
DOI:10.1021/jo00062a043

Reference yield:

: 4024-14-0
1-methyl-2-tetralone

: 147779-74-6
1-Benzyl-1-methyl-1,4-dihydronaphthaline

Guidance literature:: Multi-step reaction with 3 steps

1: 1) t-BuOK / 1) t-BuOH, 10 min, ice-cooling, 2) a) 0.5 h, cooling, b) 14 h, r.t.

2: 69 percent / aq. HCl / methanol / 36 h / Heating

3: 57 percent / MeLi / diethyl ether / 1.5 h / 0 °C

With hydrogenchloride; potassium tert-butylate; methyllithium; In methanol; diethyl ether;
DOI:10.1021/jo00062a043

Reference yield:

: 100-44-7
benzyl chloride

: 147779-74-6
1-Benzyl-1-methyl-1,4-dihydronaphthaline

Guidance literature:: Multi-step reaction with 3 steps

1: 1) t-BuOK / 1) t-BuOH, 10 min, ice-cooling, 2) a) 0.5 h, cooling, b) 14 h, r.t.

2: 69 percent / aq. HCl / methanol / 36 h / Heating

3: 57 percent / MeLi / diethyl ether / 1.5 h / 0 °C

With hydrogenchloride; potassium tert-butylate; methyllithium; In methanol; diethyl ether;
DOI:10.1021/jo00062a043