C₂₃H₂₀F₆N₄O₄

Base Information

• Chemical Name: C₂₃H₂₀F₆N₄O₄
• CAS No.: 1620412-14-7
• Molecular Formula: C₂₃H₂₀F₆N₄O₄
• Molecular Weight: 530.427

Synonyms:C₂₃H₂₀F₆N₄O₄

Chemical Property of C₂₃H₂₀F₆N₄O₄

Chemical Property:

Purity/Quality:

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Technology Process of C₂₃H₂₀F₆N₄O₄

There total 18 articles about C₂₃H₂₀F₆N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H40F6N4O4Si (1620412-13-6) → C23H20F6N4O4 (1620412-14-7)

Guidance literature:

With boron tribromide; In dichloromethane; at 0 ℃; Inert atmosphere;

Reference yield:

C24H26N2O4 → C23H20F6N4O4 (1620412-14-7)

Guidance literature:

Multi-step reaction with 11 steps

1.1: hydrogen; palladium 10% on activated carbon / methanol / 6 h / 0 - 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: bromine / dichloromethane; acetic acid / 20 °C / Inert atmosphere

4.1: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

4.2: 3.17 h / 20 - 90 °C / Inert atmosphere

5.1: hydrogenchloride / methanol; isopropyl alcohol / 20 °C

6.1: acetic anhydride / 0.5 h / 20 °C

6.2: 16 h / 60 °C

7.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 16 h / 20 °C

8.1: ammonium acetate / acetic acid / 1 h / Reflux

9.1: trifluorormethanesulfonic acid / toluene / 2 h / Reflux

10.1: sodium hydride; lithium bromide / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

10.2: 20 - 50 °C / Inert atmosphere

11.1: boron tribromide / dichloromethane / 0 °C / Inert atmosphere

With hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifluorormethanesulfonic acid; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium acetate; hydrogen; bromine; acetic anhydride; boron tribromide; sodium hydride; potassium carbonate; triphenylphosphine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium iodide; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; toluene;

Reference yield:

C17H20N2O4 → C23H20F6N4O4 (1620412-14-7)

Guidance literature:

Multi-step reaction with 10 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: bromine / dichloromethane; acetic acid / 20 °C / Inert atmosphere

3.1: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3.2: 3.17 h / 20 - 90 °C / Inert atmosphere

4.1: hydrogenchloride / methanol; isopropyl alcohol / 20 °C

5.1: acetic anhydride / 0.5 h / 20 °C

5.2: 16 h / 60 °C

6.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 16 h / 20 °C

7.1: ammonium acetate / acetic acid / 1 h / Reflux

8.1: trifluorormethanesulfonic acid / toluene / 2 h / Reflux

9.1: sodium hydride; lithium bromide / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

9.2: 20 - 50 °C / Inert atmosphere

10.1: boron tribromide / dichloromethane / 0 °C / Inert atmosphere

With hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifluorormethanesulfonic acid; di-isopropyl azodicarboxylate; ammonium acetate; bromine; acetic anhydride; boron tribromide; sodium hydride; potassium carbonate; triphenylphosphine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium iodide; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; toluene;

upstream raw materials:

C₉H₁₀N₂O₂

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