5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

Base Information

Chemical Name:5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine
CAS No.:128870-23-5
Molecular Formula:C₆₁H₆₂N₆O₁₁
Molecular Weight:1055.2
Hs Code.:

5'-O-<Bis(4-methoxyphenyl)phenylmethyl>-5-<3-<<2-<<<1-<bis(4-methoxyphenyl)phenylmethyl>-1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

Synonyms:5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

Suppliers and Price of 5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

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Technology Process of 5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

There total 6 articles about 5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 128870-19-9
N-(2-Aminoethyl)-1--1H-imidazole-4-acetamide

: 128870-22-4
5'-O--2'-deoxyuridine-5-propionic acid p-nitrophenylester

: 128870-23-5
5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

Guidance literature:: With triethylamine; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1021/jo00304a026

Reference yield:

: 3251-69-2
imidazole-4-acetic acid hydrochloride

: 128870-23-5
5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / conc. H₂SO₄ / 12 h / Heating

2: 76 percent / Et₃N / CH₂Cl₂

3: 91 percent / 48 h / Ambient temperature

4: 63 percent / Et₃N / CH₂Cl₂ / 8 h / Ambient temperature

With sulfuric acid; triethylamine; In dichloromethane;
DOI:10.1021/jo00304a026

Reference yield:

: 128870-20-2
5-(2-carbethoxyethyl)-2'-deoxyuridine

: 128870-23-5
5'-O--5-<3-<<2-<<<1--1H-imidazol-4-yl>acetyl>amino>ethyl>amino>-3-oxopropyl>-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / DCC / dimethylformamide / 1) 0 deg C, 30 min 2) r.t., 6h

2: 70 percent / pyridine / 4 h

3: 63 percent / Et₃N / CH₂Cl₂ / 8 h / Ambient temperature

With pyridine; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00304a026