tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate

Base Information

• Chemical Name: tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate
• CAS No.: 873011-41-7
• Molecular Formula: C₃₄H₃₇F₃O₈
• Molecular Weight: 630.658

Synonyms:tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate

Chemical Property of tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate

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Technology Process of tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate

There total 2 articles about tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

methyl (4'-hydroxy-2-methyl-1,1'-biphenyl-3-yl)acetate (885681-49-2) + tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate (873011-54-2) → tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate (873011-41-7)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 28.0%

→ tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate (873011-41-7)

Guidance literature:

Reference yield: 100.0%

tert-butyl 2-[(tert-butoxycarbonyl)oxy]-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate (873011-41-7) → tert-butyl 2-hydroxy-6-[({3'-[(methoxycarbonyl)methyl]-2'-methyl-1,1'-biphenyl-4-yl}oxy)methyl]-3-(trifluoromethyl)benzoate

Guidance literature:

With pyrrolidine; In tetrahydrofuran; at 40 ℃; for 1h;

upstream raw materials:

methyl (4'-hydroxy-2-methyl-1,1'-biphenyl-3-yl)acetate

tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate

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