D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI)

Base Information

Chemical Name:D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI)
CAS No.:325740-60-1
Molecular Formula:C8H11 Cl O3
Molecular Weight:190.627
Hs Code.:2932190090
Mol file:325740-60-1.mol

Synonyms:D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI)

Suppliers and Price of D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI)

Chemical Property:

PSA：43.37000
LogP:1.33950

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI)

There total 9 articles about D-erythro-Pentonic acid, 5-chloro-2,3,5-trideoxy-2-(1-methylethyl)-5-oxo-, gamma-lactone (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 325740-59-8
tetrahydro-4-isopropyl-5-oxofuran-2-carboxylic acid

: 325740-60-1
tetrahydro-4-isopropyl-5-oxofuran-2-carbonyl chloride

Guidance literature:: With oxalyl dichloride; In N,N-dimethyl-formamide; toluene; for 1h;
DOI:10.1016/S0040-4039(00)01794-9

Reference yield:

: 145589-03-3,104266-90-2
(S)-4-benzyl-3-(3-methylbutanoyl)oxazolidin-2-one

: 325740-60-1
tetrahydro-4-isopropyl-5-oxofuran-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / LIHMDS / tetrahydrofuran / -78 °C

2: 88 percent / OsO₄; NMMO / 2-methyl-propan-2-ol; acetone; H₂O

3: NaIO₄; RuCl₃*H₂O / CCl₄; acetonitrile; H₂O / 6 h

4: (COCl)2 / dimethylformamide; toluene / 1 h

5: NEt₃ / CH₂Cl₂

6: 100 percent / H₂ / Pd/C / ethyl acetate

7: (COCl)2 / toluene; dimethylformamide / 1 h

With ruthenium trichloride; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; hydrogen; 4-methylmorpholine N-oxide; triethylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)01794-9

Reference yield:

: 240821-65-2
(4S)-3-[(2S)-2-(1-methylethyl)-1-oxopent-4-en-1-yl]-4-(phenylmethyl)oxazolidin-2-one

: 325740-60-1
tetrahydro-4-isopropyl-5-oxofuran-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / OsO₄; NMMO / 2-methyl-propan-2-ol; acetone; H₂O

2: NaIO₄; RuCl₃*H₂O / CCl₄; acetonitrile; H₂O / 6 h

3: (COCl)2 / dimethylformamide; toluene / 1 h

4: NEt₃ / CH₂Cl₂

5: 100 percent / H₂ / Pd/C / ethyl acetate

6: (COCl)2 / toluene; dimethylformamide / 1 h

With ruthenium trichloride; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; hydrogen; 4-methylmorpholine N-oxide; triethylamine; palladium on activated charcoal; In tetrachloromethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)01794-9