copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin

Base Information

• Chemical Name: copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin
• CAS No.: 1384840-47-4
• Molecular Formula: C₄₉H₃₄CuN₆O
• Molecular Weight: 786.395

Synonyms:copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin

Chemical Property of copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin

Chemical Property:

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Technology Process of copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin

There total 3 articles about copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

5-[4-(2-imidazole)ethoxyl]phenyl-10,15,20-triphenyl porphyrin → copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin (1384840-47-4)

Guidance literature:

With copper dichloride; In ethanol; dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.molcata.2012.04.013

Reference yield: 93.0%

5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin + copper dichloride → copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin (1384840-47-4)

Guidance literature:

In ethanol; dichloromethane; CuCl2 (0.15 mmol) added to porphyrin ligand (0.05 mmol) in mixt. of CH2Cl2 (15 ml) and EtOH (7 ml); stirred (24 h, room temp.); monitored by TLC; filtered; chromd. on silica gel column with CH2Cl2 as eluent; elem. anal.;

DOI:10.1016/j.molcata.2012.04.013

Reference yield:

5-(4-hydroxyphenyl)-10,15,20-triphenylporphyrin → copper(II) 5-[4-(2-imidazolyl)-ethoxyl]phenyl-10,15,20-triphenylporphyrin (1384840-47-4)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

3: copper dichloride / ethanol; dichloromethane / 24 h / 20 °C

With potassium carbonate; copper dichloride; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.molcata.2012.04.013

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