4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

Base Information

Chemical Name:4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine
CAS No.:85732-94-1
Molecular Formula:C₁₇H₁₅ClN₆S
Molecular Weight:370.865
Hs Code.:

Synonyms:4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

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Chemical Property of 4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

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Technology Process of 4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

There total 5 articles about 4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 85732-81-6
4-(3,5-dimethylpyrazol-1-yl)imidazo<4,5-d>pyridazine-2-thiol

: 104-83-6
1-Chloro-4-(chloromethyl)benzene

: 85732-94-1
4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

Guidance literature:: With potassium hydroxide; at 45 ℃; for 5h;
DOI:10.1002/jhet.5570200140

Reference yield:

: 85732-75-8
6-Chloro-3-(3,5-dimethylpyrazol-1-yl)pyridazine-4,5-diamine

: 85732-94-1
4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂, 85percent ammonium hydroxide / 5percent palladium on charcoal / ethanol / 4 h / 760 Torr

2: 93 percent / sodium hydroxide/10percent HCl / pyridine / 80 °C

3: 98 percent / 1 N potassium hydroxide / 5 h / 45 °C

With hydrogenchloride; potassium hydroxide; ammonium hydroxide; sodium hydroxide; hydrogen; palladium on activated charcoal; In pyridine; ethanol;
DOI:10.1002/jhet.5570200140

Reference yield:

: 85732-74-7
3-Chloro-5-nitro-6-(3,5-dimethylpyrazol-1-yl)pyridazin-4-amine

: 85732-94-1
4-(3,5-Dimethylpyrazol-1-yl)-2-(4-chlorobenzylthio)imidazo<4,5-d>pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂ / Raney nickel T-1 / ethanol / 760 Torr / Ambient temperature

2: 98 percent / H₂, 85percent ammonium hydroxide / 5percent palladium on charcoal / ethanol / 4 h / 760 Torr

3: 93 percent / sodium hydroxide/10percent HCl / pyridine / 80 °C

4: 98 percent / 1 N potassium hydroxide / 5 h / 45 °C

With hydrogenchloride; potassium hydroxide; ammonium hydroxide; sodium hydroxide; hydrogen; palladium on activated charcoal; Raney Nickel T-1; In pyridine; ethanol;
DOI:10.1002/jhet.5570200140