allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

Base Information

Chemical Name:allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate
CAS No.:113599-76-1
Molecular Formula:C₃₂H₃₂N₂O₅
Molecular Weight:524.616
Hs Code.:

Synonyms:allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

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Chemical Property of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

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Technology Process of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

There total 5 articles about allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 113599-69-2
allyl 2-<(3S,4S)-4-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

: 113599-76-1
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/jm00401a020

Reference yield:

: 40630-84-0
allyl bromoacetate

: 113599-76-1
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent

2: LiN(SiMe₃)2 / tetrahydrofuran / -78 °C

3: tetrabutylammonium fluoride, HOAc / tetrahydrofuran

With tetrabutyl ammonium fluoride; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1039/c39870001283

Reference yield:

: 113599-63-6
allyl 2-<(3S,4S)-4-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxo-3-(tritylamino)-1-azetidinyl>acetate

: 113599-76-1
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-3-cyclopropylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: LiN(SiMe₃)2 / tetrahydrofuran / -78 °C

2: tetrabutylammonium fluoride, HOAc / tetrahydrofuran

With tetrabutyl ammonium fluoride; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1039/c39870001283