3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

Base Information

Chemical Name:3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid
CAS No.:171564-68-4
Molecular Formula:C₃₈H₃₆O₅Si
Molecular Weight:600.786
Hs Code.:

Synonyms:3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

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Chemical Property of 3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

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Technology Process of 3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

There total 7 articles about 3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 171564-67-3
3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzaldehyde

: 171564-68-4
3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; tert-butyl alcohol; at 25 ℃; for 8h;

Reference yield:

: 6908-41-4,58590-49-1
4-(methoxycarbonyl)benzyl alcohol

: 171564-68-4
3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / imidazole / dimethylformamide / 2 h / 25 °C

2: 62 percent / LiOH / dioxane; H₂O / 24 h / 25 °C

3: 96 percent / Ph₃P, DEAD / tetrahydrofuran / 0.25 h / 25 °C

4: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

5: 4-methylmorpholine N-oxide, 3 Angstroem molecular sieves, tetrapropylammonium perruthenate(VII) / acetonitrile / 0.5 h / 25 °C

6: 94 percent / 2-methyl-2-butene, aq. NaH₂PO₄, 80percent NaClO₂ / tetrahydrofuran; 2-methyl-propan-2-ol / 8 h / 25 °C

With 1H-imidazole; lithium hydroxide; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; 3 A molecular sieve; 4-methylmorpholine N-oxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; hexane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 113068-93-2
4-(tert-Butyl-diphenyl-silanyloxymethyl)-benzoic acid

: 171564-68-4
3-Benzyloxy-2-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyl]-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / Ph₃P, DEAD / tetrahydrofuran / 0.25 h / 25 °C

2: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

3: 4-methylmorpholine N-oxide, 3 Angstroem molecular sieves, tetrapropylammonium perruthenate(VII) / acetonitrile / 0.5 h / 25 °C

4: 94 percent / 2-methyl-2-butene, aq. NaH₂PO₄, 80percent NaClO₂ / tetrahydrofuran; 2-methyl-propan-2-ol / 8 h / 25 °C

With sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; 3 A molecular sieve; 4-methylmorpholine N-oxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; acetonitrile; tert-butyl alcohol;