3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Base Information

Chemical Name:3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole
CAS No.:1285572-83-9
Molecular Formula:C₁₄H₉ClFNO₄S
Molecular Weight:341.747
Hs Code.:

Synonyms:3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Suppliers and Price of 3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Chemical Property:

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Technology Process of 3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

There total 5 articles about 3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285574-99-3
3-(3-chloro-5-fluoro-4-methoxybenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole

: 1285572-83-9
3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Guidance literature:: 3-(3-chloro-5-fluoro-4-methoxybenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole; With lithium chloride; In N,N-dimethyl-formamide; at 100 ℃; for 16h;

With hydrogenchloride; In water; N,N-dimethyl-formamide;

Reference yield:

: 886497-22-9
3-chloro-5-fluoro-4-methoxybenzoic acid

: 1285572-83-9
3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

2: triethylamine / chloroform / 1.5 h / 20 °C

3: 3-chloro-benzenecarboperoxoic acid / chloroform / 16 h / 20 °C

4: lithium chloride / N,N-dimethyl-formamide / 16 h / 100 °C

With thionyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; N,N-dimethyl-formamide; In chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 886497-26-3
3-chloro-5-fluoro-4-methoxybenzoyl chloride

: 1285572-83-9
3-(3-chloro-5-fluoro-4-hydroxybenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / chloroform / 1.5 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / chloroform / 16 h / 20 °C

3: lithium chloride / N,N-dimethyl-formamide / 16 h / 100 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; In chloroform; N,N-dimethyl-formamide;