16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione

Base Information

Chemical Name:16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione
CAS No.:929683-40-9
Molecular Formula:C₃₃H₄₀N₂O₄
Molecular Weight:528.692
Hs Code.:

Synonyms:16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione

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Technology Process of 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione

There total 2 articles about 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.28%

: 929683-36-3
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxy-benzylidene]-17-oxo-5-androsten-3β-ol

: 929683-40-9
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione

Guidance literature:: With cyclohexanone; aluminum isopropoxide; In toluene; for 4h; Heating / reflux;

Reference yield:

: 151719-92-5
3-methoxy-4-(3-chloropropoxy) benzaldehyde

: 929683-40-9
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-4-androstene-3,17-dione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 2 h / 20 °C

2: 5 h / 110 - 120 °C

3: aluminum isopropoxide / toluene; hexane; diethyl ether; cyclohexanone / 4 h / Reflux

With aluminum isopropoxide; sodium hydroxide; In methanol; diethyl ether; hexane; cyclohexanone; toluene;