Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI)

Base Information

Chemical Name:Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI)
CAS No.:323180-02-5
Molecular Formula:C₉H₁₃NO₂
Molecular Weight:167.208
Hs Code.:
Mol file:323180-02-5.mol

Synonyms:Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI)

Suppliers and Price of Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI)

Chemical Property:

PSA：50.09000
LogP:1.28428

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI)

There total 2 articles about Cyclohexanecarbonitrile, 2-methoxy-1-methyl-4-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 134837-19-7
2-methoxy-1-methyl-4-((trimethylsilyl)oxy)cyclohex-3-enecarbonitrile

: 133828-05-4
1-methyl-4-oxocyclohex-2-enecarbonitrile

: 323180-02-5
2-methoxy-1-methyl-4-oxocyclohexanecarbonitrile

Guidance literature:: With ytterbium(III) triflate; In toluene; at 20 ℃; for 8h; Title compound not separated from byproducts;

Reference yield:

: 54125-02-9
danishefsky's diene

: 323180-02-5
2-methoxy-1-methyl-4-oxocyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 46 h / 123 °C / Sealed tube

2: (1S)-10-camphorsulfonic acid / diethyl ether / 48 h / 20 °C

With (1S)-10-camphorsulfonic acid; In diethyl ether; toluene; 1: Diels-Alder reaction;
DOI:10.1021/jm3003922