N^α-(4-amino-4-deoxypteroyl)-N^δ-hemiphthaloyl-L-ornithinyl-L-phenylalanine

Base Information

• Chemical Name: N^α-(4-amino-4-deoxypteroyl)-N^δ-hemiphthaloyl-L-ornithinyl-L-phenylalanine
• CAS No.: 417703-27-6
• Molecular Formula: C₃₆H₃₆N₁₀O₇
• Molecular Weight: 720.745

Synonyms:N^α-(4-amino-4-deoxypteroyl)-N^δ-hemiphthaloyl-L-ornithinyl-L-phenylalanine

Chemical Property of N^α-(4-amino-4-deoxypteroyl)-N^δ-hemiphthaloyl-L-ornithinyl-L-phenylalanine

Chemical Property:

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Technology Process of N^α-(4-amino-4-deoxypteroyl)-N^δ-hemiphthaloyl-L-ornithinyl-L-phenylalanine

There total 2 articles about N^α-(4-amino-4-deoxypteroyl)-N^δ-hemiphthaloyl-L-ornithinyl-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

phthalic anhydride (85-44-9) + Nα-(4-amino-4-deoxypteroyl)-L-ornithinyl-L-phenylalanine trifluoroacetic salt → Nα-(4-amino-4-deoxypteroyl)-Nδ-hemiphthaloyl-L-ornithinyl-L-phenylalanine (417703-27-6)

Guidance literature:

In N,N-dimethyl-formamide; for 1.5h;

DOI:10.1016/S0968-0896(01)00298-X

Reference yield: 6.8%

N-((S)-4-((S)-1-Carboxy-2-phenyl-ethylcarbamoyl)-4-{4-[(2,4-diamino-pteridin-6-ylmethyl)-formyl-amino]-benzoylamino}-butyl)-phthalamic acid; compound with trifluoro-acetic acid → Nα-(4-amino-4-deoxypteroyl)-Nδ-hemiphthaloyl-L-ornithinyl-L-phenylalanine (417703-27-6)

Guidance literature:

With sodium hydroxide; In water; at 21 ℃; for 0.5h;

DOI:10.1016/S0968-0896(01)00298-X

Reference yield:

Nα-(4-amino-4-deoxypteroyl)-Nδ-hemiphthaloyl-L-ornithinyl-L-phenylalanine (417703-27-6) → (S)-2-[[[4-carboxy-4-[[4-[[(2,4-diamino-6-pteridinyl)methyl]amino]benzoyl]amino]butyl]amino]carbonyl]benzoic acid (113857-87-7)

Guidance literature:

With bovine carboxypeptidase A; zinc(II) chloride; In various solvent(s); at 25 ℃; for 0.333333h; Enzymatic reaction;

DOI:10.1016/S0968-0896(01)00298-X

upstream raw materials:

phthalic anhydride

Downstream raw materials:

(S)-2-[[[4-carboxy-4-[[4-[[(2,4-diamino-6-pteridinyl)methyl]amino]benzoyl]amino]butyl]amino]carbonyl]benzoic acid

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