3-PHENYL-PIPERIDINE-1,2-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER

Base Information

• Chemical Name: 3-PHENYL-PIPERIDINE-1,2-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER
• CAS No.: 321983-19-1
• Molecular Formula: C₁₇H₂₃NO₄
• Molecular Weight: 305.374
• Hs Code.: 2933399090
• Mol file: 321983-19-1.mol

Synonyms:3-PHENYL-PIPERIDINE-1,2-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER;N-BOC-3-PHENYL-PIPECOLIC ACID

Chemical Property of 3-PHENYL-PIPERIDINE-1,2-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.54
• Boiling Point: 454.872°C at 760 mmHg
• PKA: 3.88±0.40(Predicted)
• Flash Point: 228.899°C
• PSA: 66.84000
• Density: 1.169g/cm³
• LogP: 3.19220

Purity/Quality:

97% ^*data from raw suppliers

3-Phenyl-piperidine-1,2-dicarboxylicacid1-tert-butylester 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-PHENYL-PIPERIDINE-1,2-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER

There total 6 articles about 3-PHENYL-PIPERIDINE-1,2-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 3-phenylpiperidine-2-carboxylic acid (130943-98-5) → 1-(tert-butoxycarbonyl)-3-phenylpiperidine-2-carboxylic acid (321983-19-1)

Guidance literature:

With sodium hydrogencarbonate; In acetone; at 20 ℃;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 3-phenylpiperidine-2-carboxylic acid (130943-98-5) → cis-1-(tert-butoxycarbonyl)-3-phenylpiperidine-2-carboxylic acid (321983-19-1)

Guidance literature:

di-tert-butyl dicarbonate; 3-phenylpiperidine-2-carboxylic acid; With sodium hydrogencarbonate; In acetone; for 12h;

With phosphoric acid; In water; acetone; pH=5.5;

Reference yield:

1-(tert-butoxycarbonyl)-3-phenylpiperidine-2-carboxylic acid (321983-19-1) → (2S,3S)-1-(tert-butoxycarbonyl)-3-phenylpiperidine-2-carboxylic acid (321983-19-1)

Guidance literature:

Supercritical conditions;

upstream raw materials:

di-tert-butyl dicarbonate

3-phenylpiperidine-2-carboxylic acid

3-phenylpyridine-2-carboxylic acid

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