5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

Base Information

Chemical Name:5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate
CAS No.:223679-08-1
Molecular Formula:C₂₃H₂₉NO₄S
Molecular Weight:415.554
Hs Code.:

Synonyms:5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

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Chemical Property of 5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

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Technology Process of 5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

There total 8 articles about 5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 223679-09-2
6-ethyl-2-phenyl-4-propyl-5-[2-(tetrahydro-pyran-2-yloxy)-ethylsulfanylcarbonyl]-nicotinic acid propyl ester

: 223679-08-1
5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

Guidance literature:: With ethanol; pyridinium p-toluenesulfonate; Heating;
DOI:10.1021/jm980550w

Reference yield:

: 54441-63-3
propyl 3-oxo-3-phenylpropanoate

: 223679-08-1
5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium acetate / ethanol / 24 h / 80 °C

2: ethanol / 80 °C

3: tetrahydro-1,4-benzoquinone / tetrahydrofuran / Heating

4: 52 percent / PPTS, EtOH / Heating

With ammonium acetate; ethanol; pyridinium p-toluenesulfonate; 1,4-Cyclohexanedione; In tetrahydrofuran; ethanol;
DOI:10.1021/jm980550w

Reference yield:

: 64074-05-1
2,2-dimethyl-5-propanoyl-1,3-dioxan-4,6-dione

: 223679-08-1
5-n-propyl 2-ethyl-4-n-propyl-3-(2-hydroxyethylsulfanylcarbonyl)-6-phenylpyridine-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / toluene / 24 h / 80 °C

2: ethanol / 80 °C

3: tetrahydro-1,4-benzoquinone / tetrahydrofuran / Heating

4: 52 percent / PPTS, EtOH / Heating

With ethanol; pyridinium p-toluenesulfonate; 1,4-Cyclohexanedione; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/jm980550w