6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

Base Information

• Chemical Name: 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide
• CAS No.: 919297-01-1
• Molecular Formula: C₂₅H₂₆F₁₇N₃O₃
• Molecular Weight: 739.473

Synonyms:6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

Chemical Property of 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

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Technology Process of 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

There total 1 articles about 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

6-N-benzyloxycarbonyl-2-N-trifluoroacetyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide (919297-00-0) → 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide (919297-01-1)

Guidance literature:

With ammonia; In ethanol; at 0 ℃; for 5h;

Reference yield: 84.0%

(3-benzyloxy-2,2-bis(benzyloxymethyl)propoxy)aceticacid (919297-51-1) + 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide (919297-01-1) → 6-N-benzyloxycarbonyl-2-N-[(3-benzyloxy-2,2-bisbenzyloxymethylpropoxy)-acetyl]-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide (919297-52-2)

Guidance literature:

With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 19h;

Reference yield: 81.0%

1-O-α-d-carbonylmethyl-(2,3,4,6-tetra-O-methyl)mannopyranose (920958-94-7) + 6-N-benzyloxycarbonyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide (919297-01-1) → 6-N-benzyloxycarbonyl-2-N-[1-O-α-d-carbonylmethyl-(2,3,4,6-tetra-O-methyl)mannopyranose]-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide (920958-95-8)

Guidance literature:

With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 19h;

upstream raw materials:

6-N-benzyloxycarbonyl-2-N-trifluoroacetyl-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

Downstream raw materials:

6-N-benzyloxycarbonyl-2-N-[(3-benzyloxy-2,2-bisbenzyloxymethylpropoxy)-acetyl]-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

6-N-benzyloxycarbonyl-2-N-[1-O-α-d-carbonylmethyl-(2,3,4,6-tetra-O-methyl)mannopyranose]-L-lysine-[(1H,1H,2H,2H-perfluorodecyl)-methyl]-amide

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