(S)-3,5-dimethylhexenone

Base Information

Chemical Name:(S)-3,5-dimethylhexenone
CAS No.:128441-46-3
Molecular Formula:C₈H₁₂O
Molecular Weight:124.183
Hs Code.:

Synonyms:(S)-3,5-dimethylhexenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3,5-dimethylhexenone

Chemical Property:

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Technology Process of (S)-3,5-dimethylhexenone

There total 8 articles about (S)-3,5-dimethylhexenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 5526-47-6
4-methyl-heptane-2,6-dione

: 128441-46-3
(S)-3,5-dimethylhexenone

Guidance literature:: With 9-epi-9-amino-9-deoxyquinine; acetic acid; In toluene; at -15 ℃; for 48 - 96h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.200802497

Reference yield:

: 284046-14-6
(5R)-1,5-dimethyl-2-cyclohexen-1-ol

: 128441-46-3
(S)-3,5-dimethylhexenone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/ol007016e

Reference yield:

: 89-82-7,90449-51-7
pulegone

: 128441-46-3
(S)-3,5-dimethylhexenone

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether

2: O₃ / CH₂Cl₂ / -78 °C

3: tetrahydrofuran

4: n-BuLi / tetrahydrofuran

5: PCC / CH₂Cl₂

With n-butyllithium; ozone; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol007016e