Os3(CO)10(μ,η3-(PPh2)C60H)

Base Information

Chemical Name:Os3(CO)10(μ,η3-(PPh2)C60H)
CAS No.:1207318-60-2
Molecular Formula:C₈₂H₁₁O₁₀Os₃P
Molecular Weight:1757.56
Hs Code.:

Synonyms:Os3(CO)10(μ,η3-(PPh2)C60H)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os3(CO)10(μ,η3-(PPh2)C60H)

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Technology Process of Os3(CO)10(μ,η3-(PPh2)C60H)

There total 2 articles about Os3(CO)10(μ,η3-(PPh2)C60H) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1207318-61-3
(C₆₀HP(C₆H₅)2)Os₃(CO)11

: 1207318-60-2
Os3(CO)10(μ,η3-(PPh2)C60H)

Guidance literature:: In toluene; under N2; Os complex in toluene heated to reflux for 2 h; cooled to roomtemp.; solvent removed under vac.; subjected to TLC (silica gel, CS2);
DOI:10.1021/om900914a

Reference yield: 54.0%

: 61817-93-4,146143-79-5,871132-66-0
bis(acetonitrile)decacarbonyltriosmium

: 159831-83-1
C₆₀HP(C₆H₅)2

: 1207318-60-2
Os3(CO)10(μ,η3-(PPh2)C60H)

Guidance literature:: In toluene; under N2; toluene added to (PPh2)C60H and Os complex; stirred at room temp. for 5 h; heated to reflux for 1 h; volatiles removed under vac.; subjected to TLC (silica gel, CS2); secondbrown band collected; crystd. from CS2-MeOH; elem. anal.;
DOI:10.1021/om900914a

Reference yield: 58.0%

: 1207318-60-2
Os3(CO)10(μ,η3-(PPh2)C60H)

: Os3(μ-H)2(μ3-η3-PPh(C6H4))(CO)9

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

Guidance literature:: In chlorobenzene; byproducts: CO; under N2; Os complex in chlorobenzene heated to reflux for 12 h; cooled to room temp.; solvent removed under vac.; subjected to TLC (silica gel, CS2); second pale yellow band collected;
DOI:10.1021/om900914a