5-AMINO-2-METHOXY-BENZAMIDE

Base Information

• Chemical Name: 5-AMINO-2-METHOXY-BENZAMIDE
• CAS No.: 22961-58-6
• Molecular Formula: C₈H₁₀N₂O₂
• Molecular Weight: 166.18
• Mol file: 22961-58-6.mol

Synonyms:5-amino-2-methoxybenzamide

Chemical Property of 5-AMINO-2-METHOXY-BENZAMIDE

Chemical Property:

• Vapor Pressure: 0.000207mmHg at 25°C
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

5-Amino-2-methoxybenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-AMINO-2-METHOXY-BENZAMIDE

There total 1 articles about 5-AMINO-2-METHOXY-BENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-methoxybenzamide (2439-77-2) → 5-amino-2-methoxybenzamide (22961-58-6)

Guidance literature:

2-methoxybenzamide; With sulfuric acid; hydroxylamine hydrochloride; In acetonitrile; at 25 ℃; for 0.166667h;

With hydrogenchloride; titanium(III) chloride; In water; acetonitrile; at 25 ℃; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.orglett.0c00598

Reference yield: 88.0%

C27H35N3O8 (1294448-77-3) + 5-amino-2-methoxybenzamide (22961-58-6) → C35H43N5O9 (1294448-74-0)

Guidance literature:

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield: 40.0%

2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzoic acid (1621060-66-9) + 5-amino-2-methoxybenzamide (22961-58-6) → N-(3-carbamoyl-4-methoxyphenyl)-2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamide

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 18h;

upstream raw materials:

2-methoxybenzamide

Downstream raw materials:

3'-Methoxy-2'-N-Methylcarbamyloxanilic acid ethyl ester

C₂₇H₃₆N₄O₇

C₂₂H₂₈N₄O₅

C₄₉H₆₁N₇O₁₂

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