3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

Base Information

Chemical Name:3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate
CAS No.:1398574-81-6
Molecular Formula:C₄₉H₅₂O₁₀
Molecular Weight:800.946
Hs Code.:

Synonyms:3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

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Chemical Property of 3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

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Technology Process of 3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

There total 11 articles about 3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1331828-93-3
4-((3-hydroxyphenoxy)carbonyl)phenyl 4-(heptyloxy)benzoate

: 151792-22-2
4-[(4-[(1R)-1-methylheptyl]oxybenzoyl)oxy]benzoic acid

: 1398574-81-6
3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

Guidance literature:: 4-((3-hydroxyphenoxy)carbonyl)phenyl 4-(heptyloxy)benzoate; 4-[(4-[(1R)-1-methylheptyl]oxybenzoyl)oxy]benzoic acid; With dicyclohexyl-carbodiimide; In dichloromethane; for 0.166667h;

With dmap; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/chem.201200057

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1398574-81-6
3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine / tetrahydrofuran / 0.25 h / 0 °C

1.2: 8 h / 0 - 20 °C

2.1: water; potassium hydroxide / tetrahydrofuran / 8 h / 80 °C

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 10 h / 20 °C

4.1: palladium 10% on activated carbon / ethanol; cyclohexene / 8 h / Reflux

5.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

5.2: 16 h / 20 °C

With dmap; palladium 10% on activated carbon; water; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; cyclohexene; 1.1: Mitsunobu reaction / 1.2: Mitsunobu reaction;
DOI:10.1002/chem.201200057

Reference yield:

: 151792-21-1
C₂₉H₃₂O₅

: 1398574-81-6
3-[(4-{[4-(heptyloxy)benzoyl]oxy}benzoyl)oxy]phenyl 4-[(4-{[(1R)-1-methylheptyl]oxy}benzoyl)oxy] benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon / ethanol; cyclohexene / 8 h / Reflux

2.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

2.2: 16 h / 20 °C

With palladium 10% on activated carbon; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; cyclohexene;
DOI:10.1002/chem.201200057