(E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

Base Information

Chemical Name:(E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine
CAS No.:944730-06-7
Molecular Formula:C₂₄H₂₃NO₃
Molecular Weight:373.452
Hs Code.:

Synonyms:(E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

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Technology Process of (E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

There total 7 articles about (E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.9%

: 944729-90-2
diethyl (7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)methylphosphonate

: 100-10-7
4-dimethylamino-benzaldehyde

: 944730-06-7
(E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

Guidance literature:: diethyl (7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)methylphosphonate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

4-dimethylamino-benzaldehyde; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Further stages.;
DOI:10.1002/ardp.200600146

Reference yield:

: 944729-84-4
4-(benzyloxy)-6-(chloromethyl)benzo[d][1,3]dioxole

: 944730-06-7
(E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 8 h / 140 °C

2.1: NaH / dimethylformamide / 1 h / 20 °C

2.2: 52.9 percent / dimethylformamide / 6 h / 20 °C

With sodium hydride; In N,N-dimethyl-formamide; 1.1: Michaelis-Arbuzov reaction / 2.2: Wittig-Horner reaction;
DOI:10.1002/ardp.200600146

Reference yield:

: 99-24-1
methyl galloate

: 944730-06-7
(E)-4-(2-(7-(benzyloxy)benzo[d][1,3]dioxol-5-yl)vinyl)-N,N-dimethylbenzenamine

Guidance literature:: Multi-step reaction with 6 steps

1.1: aq. Na₂B₄O₇*10H₂O; K₂CO₃ / dimethylformamide / 0.5 h / 20 °C

1.2: dimethylformamide / 20 °C

2.1: K₂CO₂ / dimethylformamide / 4 h / Heating

3.1: 86.7 percent / NaBH₄; I₂ / tetrahydrofuran / 8 h / Heating

4.1: 95.5 percent / Et₃N; SOCl₂ / 1,2-dichloro-ethane / 6 h / 20 °C

5.1: 8 h / 140 °C

6.1: NaH / dimethylformamide / 1 h / 20 °C

6.2: 52.9 percent / dimethylformamide / 6 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; iodine; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide; 5.1: Michaelis-Arbuzov reaction / 6.2: Wittig-Horner reaction;
DOI:10.1002/ardp.200600146