dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate

Base Information

• Chemical Name: dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate
• CAS No.: 147072-61-5
• Molecular Formula: C₂₆H₃₁O₁₁P
• Molecular Weight: 550.499
• Mol file: 147072-61-5.mol

Synonyms:dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate

Chemical Property of dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate

There total 5 articles about dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

phosphoric acid dibenzyl ester (1623-08-1) + 1-O-trifluoroacetyl-2,3,4-tri-O-acetyl-α-L-rhamnopyranose (171072-42-7) → dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate (147072-61-5)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1080/00397919508011798

Reference yield: 78.0%

phosphoric acid dibenzyl ester (1623-08-1) + 2,3,4-tri-O-acetyl-L-rhamnopyranosyl trichloroacetimidate (113893-72-4) → dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate (147072-61-5)

Guidance literature:

In dichloromethane; for 1h; Ambient temperature;

Reference yield:

phosphoric acid dibenzyl ester (1623-08-1) + 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl bromide (5158-64-5) → dibenzyl 2,3,4-tri-O-acetyl-6-deoxy-α-L-talopyranosyl phosphate (147072-61-5)

Guidance literature:

With 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃;

DOI:10.1016/j.carres.2008.01.046

upstream raw materials:

phosphoric acid dibenzyl ester

2,3,4-tri-O-acetyl-L-rhamnopyranosyl trichloroacetimidate

1-O-trifluoroacetyl-2,3,4-tri-O-acetyl-α-L-rhamnopyranose

2,3,4-tri-O-acetyl-L-rhamnopyranose