11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

Base Information

Chemical Name:11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate
CAS No.:911366-00-2
Molecular Formula:C₂₆H₄₁NO₄S
Molecular Weight:463.682
Hs Code.:

Synonyms:11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

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Chemical Property of 11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

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Technology Process of 11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

There total 5 articles about 11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911365-95-2
11-acetylsulfanyl-undecyl bromoacetate

: 911366-00-2
11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: ethyl acetate / 72 h / 20 °C

2: Et₃N / benzene / 0.25 h

3: 0.45 g / benzene / 18 h / 20 °C

With triethylamine; In ethyl acetate; benzene;
DOI:10.1021/ja063562c

Reference yield:

: (11-acetylsulfanyl-undecyloxycarbonymethyl)-triphenylphosphonium bromide

: 911366-00-2
11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / benzene / 0.25 h

2: 0.45 g / benzene / 18 h / 20 °C

With triethylamine; In benzene;
DOI:10.1021/ja063562c

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 911366-00-2
11-acetylsulfanyl-undecyl E-3-(4-diethylamino-2-hydroxy-phenyl)propenoate

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / dimethylformamide / 20 h / 20 °C

2: pyridine; DMAP / CH₂Cl₂ / 0.5 h / 0 °C

3: ethyl acetate / 72 h / 20 °C

4: Et₃N / benzene / 0.25 h

5: 0.45 g / benzene / 18 h / 20 °C

With pyridine; dmap; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ja063562c