ophiocarpine acetate β-N-methyl chloride

Base Information

• Chemical Name: ophiocarpine acetate β-N-methyl chloride
• CAS No.: 82864-47-9
• Molecular Formula: C₂₃H₂₆NO₆*Cl
• Molecular Weight: 447.916

Synonyms:ophiocarpine acetate β-N-methyl chloride

Chemical Property of ophiocarpine acetate β-N-methyl chloride

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Technology Process of ophiocarpine acetate β-N-methyl chloride

There total 1 articles about ophiocarpine acetate β-N-methyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7,8-dihydroberberine (483-15-8) → ophiocarpine acetate β-N-methyl chloride (82864-47-9)

Guidance literature:

Multi-step reaction with 5 steps

1: m-chloroperbenzoic acid / CH₂Cl₂ / from -70 deg C to RT

2: NaBH₄ / ethanol; H₂O

3: 160 mg / Ambient temperature

4: 370 mg / acetone / Ambient temperature

5: AgCl / methanol

With sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; silver(I) chloride; In methanol; ethanol; dichloromethane; water; acetone;

DOI:10.1021/jo00143a021

upstream raw materials:

7,8-dihydroberberine

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