2-Iododibenzothiophene

Base Information

Chemical Name:2-Iododibenzothiophene
CAS No.:177586-41-3
Molecular Formula:C₁₂H₇IS
Molecular Weight:310.158
Hs Code.:
Mol file:177586-41-3.mol

Synonyms:2-iododibenzo[b,d]thiophene

Suppliers and Price of 2-Iododibenzothiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Iododibenzothiophene
2.5mg
$ 45.00

TCI Chemical
2-Iododibenzothiophene >98.0%(GC)
200mg
$ 66.00

TCI Chemical
2-Iododibenzothiophene >98.0%(GC)
1g
$ 227.00

Crysdot
2-Iododibenzo[b,d]thiophene 95+%
5g
$ 544.00

AK Scientific
2-Iododibenzothiophene
1g
$ 368.00

AK Scientific
2-Iododibenzothiophene
200mg
$ 143.00

Total 13 raw suppliers

Chemical Property of 2-Iododibenzothiophene

Chemical Property:

Melting Point:89.0 to 93.0 °C
Boiling Point:408.2±18.0 °C(Predicted)
Density:1.832±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

2-Iododibenzothiophene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 2-Iododibenzothiophene?is a thiophene derivative and is used in pharmaceutical synthesis.

Technology Process of 2-Iododibenzothiophene

There total 2 articles about 2-Iododibenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 132-65-0
dibenzothiophene

: 177586-41-3
2-iododibenzo[b,d]thiophene

Guidance literature:: With sulfuric acid; iodine; periodic acid; In water; acetic acid; at 60 ℃; for 4.5h;

Reference yield:

: 177586-41-3
2-iododibenzo[b,d]thiophene

Guidance literature:: nach Sandmeyer;

Reference yield: 93.0%

: 3262-89-3
triphenylboroxine

: 177586-41-3
2-iododibenzo[b,d]thiophene

: 3776-91-8
2-phenyldibenzo[b,d]thiophene

Guidance literature:: triphenylboroxine; With potassium tert-butylate; zinc(II) chloride; In 1-methyl-pyrrolidin-2-one; at 23 ℃; for 1h; Inert atmosphere; Glovebox;

2-iododibenzo[b,d]thiophene; In 1-methyl-pyrrolidin-2-one; at 110 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1002/anie.201802813