Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

Base Information

Chemical Name:Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside
CAS No.:175980-94-6
Molecular Formula:C₂₈H₃₈O₆SSi
Molecular Weight:530.758
Hs Code.:

Synonyms:Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

Chemical Property:

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Technology Process of Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

There total 5 articles about Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 613-90-1
benzoyl cyanide

: 175980-94-6
Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) triethylamine / 1.) pyridine, -17 degC

2: hydrazinium acetate / dimethylformamide

3: 1.) trifluoromethanesulfonic anhydride; 2.) tetrabutylammonium nitrite / 1.) pyridine

With hydrazinium monoacetate; trifluoromethanesulfonic acid anhydride; triethylamine; tetrabutylammonium nitrite; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00061-5

Reference yield:

: 175980-93-5
(2S,4aR,6S,7R,8R,8aR)-6-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

: 175980-94-6
Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) triethylamine / 1.) pyridine, -17 degC

2: hydrazinium acetate / dimethylformamide

3: 1.) trifluoromethanesulfonic anhydride; 2.) tetrabutylammonium nitrite / 1.) pyridine

With hydrazinium monoacetate; trifluoromethanesulfonic acid anhydride; triethylamine; tetrabutylammonium nitrite; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00061-5

Reference yield:

: 175981-00-7
Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranoside

: 175980-94-6
Thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazinium acetate / dimethylformamide

2: 1.) trifluoromethanesulfonic anhydride; 2.) tetrabutylammonium nitrite / 1.) pyridine

With hydrazinium monoacetate; trifluoromethanesulfonic acid anhydride; tetrabutylammonium nitrite; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00061-5