N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

Base Information

Chemical Name:N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide
CAS No.:371156-94-4
Molecular Formula:C₂₄H₂₃NO₃S
Molecular Weight:405.518
Hs Code.:

Synonyms:N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

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Technology Process of N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

There total 6 articles about N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 371156-89-7
N-(3,4-dimethoxyphenyl)methyl-1-phenyl-(2-phenylsulfinyl)ethylformamide

: 371156-94-4
N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

: (3S^*,4R^*)-2-formyl-6,7-dimethoxy-3-phenyl-4-phenylsulfanyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With boron trifluoride diethyl etherate; trifluoroacetic anhydride; In benzene; at 20 ℃; for 3h;
DOI:10.1248/cpb.49.979

Reference yield:

: 16222-10-9
1-phenyl-2-(phenylthio)ethanone

: 371156-94-4
N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

Guidance literature:: Multi-step reaction with 5 steps

1: Ti(O-iPr)4 / 3 h / 80 °C

2: NaBH₄ / methanol / 1 h / 20 °C

3: 96 percent / formic acid / 1 h / 60 °C

4: 97 percent / aq. NaIO₄ / methanol / 1.5 h / 20 °C

5: 53 percent / TFAA / benzene / 24 h / 20 °C

With titanium(IV) isopropylate; sodium tetrahydroborate; sodium periodate; formic acid; trifluoroacetic anhydride; In methanol; benzene;
DOI:10.1248/cpb.49.979

Reference yield:

: 5763-61-1
3,4-dimethoxybenzylamine

: 371156-94-4
N-(3,4-dimethoxyphenyl)methyl-N-[(E)-1-phenyl-2-(phenylsulfanyl)ethenyl]formamide

Guidance literature:: Multi-step reaction with 5 steps

1: Ti(O-iPr)4 / 3 h / 80 °C

2: NaBH₄ / methanol / 1 h / 20 °C

3: 96 percent / formic acid / 1 h / 60 °C

4: 97 percent / aq. NaIO₄ / methanol / 1.5 h / 20 °C

5: 53 percent / TFAA / benzene / 24 h / 20 °C

With titanium(IV) isopropylate; sodium tetrahydroborate; sodium periodate; formic acid; trifluoroacetic anhydride; In methanol; benzene;
DOI:10.1248/cpb.49.979