C₃₅H₃₅FN₄O₇

Base Information

Chemical Name:C₃₅H₃₅FN₄O₇
CAS No.:1403851-19-3
Molecular Formula:C₃₅H₃₅FN₄O₇
Molecular Weight:642.684
Hs Code.:

C<sub>35</sub>H<sub>35</sub>FN<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₅H₃₅FN₄O₇

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Chemical Property of C₃₅H₃₅FN₄O₇

Chemical Property:

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Technology Process of C₃₅H₃₅FN₄O₇

There total 4 articles about C₃₅H₃₅FN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154-08-5,343-91-9,97749-24-1
DL-5-fluorotryptophan

: 1403851-19-3
C₃₅H₃₅FN₄O₇

Guidance literature:: Multi-step reaction with 5 steps

1: chloro-trimethyl-silane / 20 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 1 h / 85 °C

4: hydrogen / palladium 10% on activated carbon / methanol / 1 h

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

With chloro-trimethyl-silane; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 5-fluoro-DL-tryptophan methyl ester hydrochloride

: 1403851-19-3
C₃₅H₃₅FN₄O₇

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 1 h / 85 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 1 h

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 1403851-18-2
C₂₆H₃₀FN₃O₅

: 1403851-19-3
C₃₅H₃₅FN₄O₇

Guidance literature:: Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 1 h / 85 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 1 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;