3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

Base Information

Chemical Name:3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran
CAS No.:1427216-08-7
Molecular Formula:C₁₇H₁₃IO₅
Molecular Weight:424.192
Hs Code.:

Synonyms:3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

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Chemical Property of 3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

Chemical Property:

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Technology Process of 3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

There total 7 articles about 3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1427216-05-4
5,6-methylenedioxy-3-hydroxymethylbenzofuran

: 41046-70-2
2-iodo-5-methoxyphenol

: 1427216-08-7
3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

Guidance literature:: With diisopropyl (E)-azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 2h; Reflux;
DOI:10.1080/00397911.2012.661910

Reference yield: 36.0%

: 1-(benzo[d][1,3]dioxol-5-yloxy)-3-(2-iodo-5-methoxyphenoxy)propan-2-one

: 1427216-08-7
3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

Guidance literature:: With boron trichloride; In dichloromethane; at -78 ℃; for 0.5h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c6ob01451h

Reference yield:

: 533-31-3
Sesamol

: 1427216-08-7
3-((2-iodo-5-methoxyphenoxy)methyl)-5,6-methylene-dioxybenzofuran

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium chloride; triethylamine / acetonitrile / 6 h / Reflux; Inert atmosphere

2: tetrafluoroboric acid diethyl ether / dichloromethane / 1 h / 25 - 30 °C / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane; hexane / -78 - 20 °C

4: triphenylphosphine; diisopropyl (E)-azodicarboxylate / tetrahydrofuran / 2 h / Reflux

With tetrafluoroboric acid diethyl ether; diisobutylaluminium hydride; diisopropyl (E)-azodicarboxylate; triethylamine; triphenylphosphine; magnesium chloride; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1080/00397911.2012.661910