Technology Process of C18H17NO2
There total 5 articles about C18H17NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
for 3h;
under 760.051 Torr;
DOI:10.1021/ol400223d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / dimethyl sulfoxide / 20 °C
2: sodium azide; boron trifluoride diethyl etherate; trifluoroacetic acid / dichloromethane / 0.5 h / 0 - 20 °C
3: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 760.05 Torr
With
sodium azide; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; potassium carbonate; trifluoroacetic acid;
In
ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol400223d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran; mineral oil / 16 h / Reflux
2: potassium carbonate / dimethyl sulfoxide / 20 °C
3: sodium azide; boron trifluoride diethyl etherate; trifluoroacetic acid / dichloromethane / 0.5 h / 0 - 20 °C
4: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 760.05 Torr
With
sodium azide; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ol400223d
