C₂₅H₃₂O₄

Base Information

Chemical Name:C₂₅H₃₂O₄
CAS No.:80878-26-8
Molecular Formula:C₂₅H₃₂O₄
Molecular Weight:396.527
Hs Code.:

C<sub>25</sub>H<sub>32</sub>O<sub>4</sub>

Synonyms:C₂₅H₃₂O₄

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Chemical Property of C₂₅H₃₂O₄

Chemical Property:

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Technology Process of C₂₅H₃₂O₄

There total 8 articles about C₂₅H₃₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 80890-22-8
C₂₅H₃₂O₃

: 80878-26-8
C₂₅H₃₂O₄

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; In benzene; Ambient temperature;
DOI:10.1021/ja00370a067

Reference yield:

: 80878-24-6
(3S,3aS,4R,7S,7aR,9R)-7a-Acetyl-3-benzyloxy-7-methoxymethoxy-4,9-dimethyl-octahydro-4,7-ethano-inden-5-one

: 80878-26-8
C₂₅H₃₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1: 67 percent / tetrahydrofuran; diethyl ether / -40 °C

2: 79 percent / PCC / CH₂Cl₂

3: 82 percent / tetrahydrofuran / -93 - -80 °C

4: 88 percent / MnO₂ / CH₂Cl₂

5: 61 percent / hydrogen / 10percent Pd/Al₂O₃, MnO / various solvent(s); ethyl acetate / 760 Torr

6: 92 percent / K₂CO₃ / methanol

7: POCl₃, DMAP / CH₂Cl₂; pyridine / 35 °C

8: 80 percent / CF₃COOH / CH₂Cl₂ / Ambient temperature

9: 97 percent / t-BuOOH, VO(acac)2 / benzene / Ambient temperature

With tert.-butylhydroperoxide; dmap; manganese(IV) oxide; bis(acetylacetonate)oxovanadium; hydrogen; potassium carbonate; pyridinium chlorochromate; trifluoroacetic acid; trichlorophosphate; palladium/alumina; manganese(II) oxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; ethyl acetate; benzene;
DOI:10.1021/ja00370a067

Reference yield:

: (3R,3aS,4S,7R,7aR,9S)-3-Benzyloxy-7a-((E)-3-hydroxy-1-methyl-but-1-enyl)-7-methoxymethoxy-4,9-dimethyl-octahydro-4,7-ethano-inden-5-one

: 80878-26-8
C₂₅H₃₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / MnO₂ / CH₂Cl₂

2: 61 percent / hydrogen / 10percent Pd/Al₂O₃, MnO / various solvent(s); ethyl acetate / 760 Torr

3: 92 percent / K₂CO₃ / methanol

4: POCl₃, DMAP / CH₂Cl₂; pyridine / 35 °C

5: 80 percent / CF₃COOH / CH₂Cl₂ / Ambient temperature

6: 97 percent / t-BuOOH, VO(acac)2 / benzene / Ambient temperature

With tert.-butylhydroperoxide; dmap; manganese(IV) oxide; bis(acetylacetonate)oxovanadium; hydrogen; potassium carbonate; trifluoroacetic acid; trichlorophosphate; palladium/alumina; manganese(II) oxide; In pyridine; methanol; dichloromethane; ethyl acetate; benzene;
DOI:10.1021/ja00370a067