C₃₃H₅₁BrO₄Si₂

Base Information

Chemical Name:C₃₃H₅₁BrO₄Si₂
CAS No.:1266178-36-2
Molecular Formula:C₃₃H₅₁BrO₄Si₂
Molecular Weight:647.841
Hs Code.:

C<sub>33</sub>H<sub>51</sub>BrO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₃H₅₁BrO₄Si₂

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Chemical Property of C₃₃H₅₁BrO₄Si₂

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Technology Process of C₃₃H₅₁BrO₄Si₂

There total 6 articles about C₃₃H₅₁BrO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1266178-99-7
C₃₃H₅₃BrO₄Si₂

: 1266178-36-2
C₃₃H₅₁BrO₄Si₂

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201005850

Reference yield:

: C₃₀H₄₆O₃Si₂

: 1266178-36-2
C₃₃H₅₁BrO₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: silver nitrate; calcium carbonate / water; acetone / 4 h / Inert atmosphere; Darkness

2: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

3: water; sodium hydrogencarbonate / methanol / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

5: trichloroacetic acid / tetrahydrofuran; water / Inert atmosphere

6: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; water; sodium hydrogencarbonate; Dess-Martin periodane; silver nitrate; calcium carbonate; trichloroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 6: Dess-Martin oxidation;
DOI:10.1002/anie.201005850

Reference yield:

: 1266178-31-7
C₃₀H₄₆O₃Si₂

: 1266178-36-2
C₃₃H₅₁BrO₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

2: water; sodium hydrogencarbonate / methanol / Inert atmosphere

3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4: trichloroacetic acid / tetrahydrofuran; water / Inert atmosphere

5: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; water; sodium hydrogencarbonate; Dess-Martin periodane; trichloroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; 5: Dess-Martin oxidation;
DOI:10.1002/anie.201005850