C₃₄H₃₂Cl₂N₄O₄

Base Information

Chemical Name:C₃₄H₃₂Cl₂N₄O₄
CAS No.:1369595-25-4
Molecular Formula:C₃₄H₃₂Cl₂N₄O₄
Molecular Weight:631.558
Hs Code.:

C<sub>34</sub>H<sub>32</sub>Cl<sub>2</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₃₄H₃₂Cl₂N₄O₄

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Chemical Property of C₃₄H₃₂Cl₂N₄O₄

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Technology Process of C₃₄H₃₂Cl₂N₄O₄

There total 10 articles about C₃₄H₃₂Cl₂N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-25-4
C₃₄H₃₂Cl₂N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid / ethanol / 15 h / 90 °C

2: polyphosphoric acid / 2 h / 110 °C

3: N-chloro-succinimide / tetrahydrofuran; dichloromethane / 3 h / 0 - 20 °C

4: toluene-4-sulfonic acid / o-xylene / 15 h / 170 °C

5: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 4 h / 95 °C / Inert atmosphere

6: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 6 h / 95 °C / Inert atmosphere

With N-chloro-succinimide; potassium acetate; sodium carbonate; toluene-4-sulfonic acid; acetic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; o-xylene;

Reference yield:

: 1007882-59-8
(S)-2-(4-bromo-1H-imidazol-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: C₂₈H₂₆BCl₂NO₄

: 1369595-25-4
C₃₄H₃₂Cl₂N₄O₄

Guidance literature:: With sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; at 95 ℃; for 6h; Inert atmosphere;

Reference yield:

: 69610-40-8
N-(tert-butoxycarbonyl)-L-prolinol

: 1369595-25-4
C₃₄H₃₂Cl₂N₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / Cooling with ice

2.1: ammonia / methanol / 0.5 h / 20 - 30 °C

2.2: 16 h / 20 - 60 °C

3.1: N-Bromosuccinimide / dichloromethane / 1.25 h / Cooling with ice

4.1: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 6 h / 95 °C / Inert atmosphere

With N-Bromosuccinimide; oxalyl dichloride; ammonia; sodium carbonate; dimethyl sulfoxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dichloromethane;