1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzofluorene trifluoromethanesulfonate

Base Information

• Chemical Name: 1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzo
• Molecular Formula: CF₃O₃S*C₃₄H₂₆NS
• Molecular Weight: 629.724

Synonyms:1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzofluorene trifluoromethanesulfonate

Chemical Property of 1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzo

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

There total 3 articles about 1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzofluorene trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

Trifluoro-methanesulfonate2,4-diphenyl-5,6-dihydro-1-oxonia-11-thia-benzo[a]fluorene; (88047-17-0) + benzylamine (100-46-9) → 1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzofluorene trifluoromethanesulfonate (88047-26-1)

Guidance literature:

With triethylamine; In dichloromethane; for 0.5h;

DOI:10.1039/P29830001463

Reference yield:

2,3-dihydrodibenzo[b,d]thiophen-4(1H)-one (24444-98-2) → 1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzofluorene trifluoromethanesulfonate (88047-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / 1.5 h / melt, then heating

2: 86 percent / triethylamine / CH₂Cl₂ / 0.5 h

With triethylamine; In dichloromethane;

DOI:10.1039/P29830001463

Reference yield:

1,3-diphenyl-propen-3-one (614-47-1) → 1-benzyl-5,6-dihydro-2,4-diphenyl-1-azonia-11-thiabenzofluorene trifluoromethanesulfonate (88047-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / 1.5 h / melt, then heating

2: 86 percent / triethylamine / CH₂Cl₂ / 0.5 h

With triethylamine; In dichloromethane;

DOI:10.1039/P29830001463

upstream raw materials:

Trifluoro-methanesulfonate2,4-diphenyl-5,6-dihydro-1-oxonia-11-thia-benzo[a]fluorene;

benzylamine

2,3-dihydrodibenzo[b,d]thiophen-4(1H)-one

1,3-diphenyl-propen-3-one

Downstream raw materials:

(2-methyl-2-nitropropyl)benzene

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