3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

Base Information

Chemical Name:3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester
CAS No.:1268862-01-6
Molecular Formula:C₂₄H₂₉NO₅
Molecular Weight:411.498
Hs Code.:

Synonyms:3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

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Chemical Property of 3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

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Technology Process of 3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

There total 5 articles about 3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1268861-77-3
6-(4-benzyloxy-phenyl)-morpholin-3-one

: 1268862-01-6
3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 4254-67-5
2-bromo-1-(4-benzyloxyphenyl)-1-ethanone

: 1268862-01-6
3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / tetrabutylammomium bromide / dichloromethane; water / 4 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2.33 h / 0 - 20 °C

3: triethylamine / dichloromethane; methanol / -10 - 20 °C

4: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C

5: sodium hydroxide / tetrahydrofuran / 2 h / 20 °C

With lithium aluminium tetrahydride; sodium azide; potassium tert-butylate; triethylamine; sodium hydroxide; tetrabutylammomium bromide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 56443-72-2
4-benzyloxy-α-(aminomethyl)benzyl alcohol

: 1268862-01-6
3-[2-(4-benzyloxy-phenyl)-5-oxo-morpholin-4-yl]-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane; methanol / -10 - 20 °C

2: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C

3: sodium hydroxide / tetrahydrofuran / 2 h / 20 °C

With potassium tert-butylate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;