1-<1-(N¹,N¹-Dimethyl-N²-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff

Base Information

• Chemical Name: 1-<1-(N¹,N¹-Dimethyl-N²-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff
• CAS No.: 73766-21-9
• Molecular Formula: C₂₀H₂₆N₄O₃S
• Molecular Weight: 402.517

Synonyms:1-<1-(N¹,N¹-Dimethyl-N²-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff

Chemical Property of 1-<1-(N¹,N¹-Dimethyl-N²-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff

Chemical Property:

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Technology Process of 1-<1-(N¹,N¹-Dimethyl-N²-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff

There total 2 articles about 1-<1-(N¹,N¹-Dimethyl-N²-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

C14H19N3O3S (54856-34-7) + aniline (62-53-3) → phenyl toluenesulfonamide (68-34-8) + 5-(Dimethylamino)-3,4-dihydro-4,4-dimethyl-2H-imidazol-2-on (73766-15-1) + 1-<1-(N1,N1-Dimethyl-N2-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff (73766-21-9)

Guidance literature:

In dichloromethane; Ambient temperature;

Reference yield:

Tosyl isocyanate (4083-64-1) → 1-<1-(N1,N1-Dimethyl-N2-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff (73766-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / diethyl ether / Ambient temperature

2: 49 percent / CH₂Cl₂ / Ambient temperature

In diethyl ether; dichloromethane;

Reference yield: 100.0%

1-<1-(N1,N1-Dimethyl-N2-p-tolylsulfonylamidino)-1-methylethyl>-3-phenylharnstoff (73766-21-9) → 5,5-Dimethyl-3-phenyl-4-(p-tolylsulfonylimino)-2-imidazolidinon (73766-23-1)

Guidance literature:

at 80 ℃;

upstream raw materials:

C₁₄H₁₉N₃O₃S

aniline

Tosyl isocyanate

Downstream raw materials:

5,5-Dimethyl-3-phenyl-4-(p-tolylsulfonylimino)-2-imidazolidinon

5,5-Dimethyl-4-(methylimino)-3-phenyl-2-imidazolidinon

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