2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI)

Base Information

Chemical Name:2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI)
CAS No.:314264-81-8
Molecular Formula:C₇H₈O₄
Molecular Weight:156.138
Hs Code.:
Mol file:314264-81-8.mol

Synonyms:2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI)

Suppliers and Price of 2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI)

Chemical Property:

PSA：52.60000
LogP:0.03110

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI)

There total 4 articles about 2-Furancarboxylicacid,tetrahydro-2-methyl-4-methylene-5-oxo-,(2R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154492-32-7
(+/-)-ethyl 2-methyl-4-methylene-tetrahydro-5-oxo-2-furancarboxylate

: 314264-83-0,314264-81-8
(+)-2-methyl-4-methylene-tetrahydro-5-oxo-2-furancarboxylic acid

Guidance literature:: With phosphate buffer; porcine pancreatic lipase; In acetone; at 20 ℃; for 0.5h; pH=7.4;
DOI:10.1016/S0957-4166(00)00309-8

Reference yield:

: 389063-31-4
4-ethoxycarbonyl-4-hydroxy-2-methylidenepentanoic acid

: 314264-83-0,314264-81-8
(+)-2-methyl-4-methylene-tetrahydro-5-oxo-2-furancarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH / toluene / 110 °C

2: Porcine pancreatic lipase; 0.1M aq. phosphate buffer / acetone / 0.5 h / 20 °C / pH 7.4

With phosphate buffer; porcine pancreatic lipase; toluene-4-sulfonic acid; In acetone; toluene; 1: Cyclization / 2: Hydrolysis;
DOI:10.1016/S0957-4166(00)00309-8

Reference yield:

: 154492-32-7
(+/-)-ethyl 2-methyl-4-methylene-tetrahydro-5-oxo-2-furancarboxylate

: 314264-81-8
(-)-2-methyl-4-methylene-tetrahydro-5-oxo-2-furancarboxylic acid

Guidance literature:: With phosphate buffer; Candida rugosa lipase; In acetone; at 20 ℃; for 1.83333h; pH=7.4;
DOI:10.1016/S0957-4166(00)00309-8