ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

Base Information

Chemical Name:ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate
CAS No.:1453495-28-7
Molecular Formula:C₁₉H₂₈N₆O₂
Molecular Weight:372.47
Hs Code.:

Synonyms:ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

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Technology Process of ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

There total 3 articles about ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: C₁₉H₂₆N₆O₄

: 1453495-28-7
ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

Guidance literature:: With tin(II) chloride dihdyrate; In methanol; for 12h; Reflux;
DOI:10.1055/s-0033-1338953

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 1453495-28-7
ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilylazide / methanol / 48 h / 20 °C

2: tin(II) chloride dihdyrate / methanol / 12 h / Reflux

With tin(II) chloride dihdyrate; trimethylsilylazide; In methanol;
DOI:10.1055/s-0033-1338953

Reference yield:

: 141-97-9
ethyl acetoacetate

: 88-74-4
2-nitro-aniline

: 1453495-28-7
ethyl 3-[(2-aminophenyl)amino]-3-(1-cyclohexyl-1H-tetrazol-5-yl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilylazide / methanol / 48 h / 20 °C

2: tin(II) chloride dihdyrate / methanol / 12 h / Reflux

With tin(II) chloride dihdyrate; trimethylsilylazide; In methanol;
DOI:10.1055/s-0033-1338953