N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine

Base Information

• Chemical Name: N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine
• CAS No.: 132611-18-8
• Molecular Formula: C₂₀H₂₁N₅O₃
• Molecular Weight: 379.418

Synonyms:N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine

Chemical Property of N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine

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Technology Process of N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine

There total 3 articles about N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N1-methoxycarbonyl-N2-benzyl-N2-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine (132611-17-7) → N1-methoxycarbonyl-N2-benzyl-N2-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine (132611-18-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 1.5h; under 2327.2 Torr;

DOI:10.1055/s-1990-27103

Reference yield:

N1-benzyl-N2-methoxycarbonylhydrazine (69353-11-3) → N1-methoxycarbonyl-N2-benzyl-N2-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine (132611-18-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) 1,1'-carbonyldiimidazole / 1) THF, reflux, ca. 1.5 h 2) r.t., 4-5 h

2: 73 percent / H₂ / Pd-C (10percent) / methanol / 1.5 h / 2327.2 Torr

With hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol;

DOI:10.1055/s-1990-27103

Reference yield:

5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid (69195-96-6) → N1-methoxycarbonyl-N2-benzyl-N2-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine (132611-18-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) 1,1'-carbonyldiimidazole / 1) THF, reflux, ca. 1.5 h 2) r.t., 4-5 h

2: 73 percent / H₂ / Pd-C (10percent) / methanol / 1.5 h / 2327.2 Torr

With hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol;

DOI:10.1055/s-1990-27103

upstream raw materials:

N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine

N¹-benzyl-N²-methoxycarbonylhydrazine

5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid

Downstream raw materials:

7-benzyl-3,4,6,7-tetrahydroimidazo<4,5-e><1,2,4>triazepine-5,8-dione

3,7-dibenzyl-3,4,6,7-tetrahydroimidazo<4,5-e><1,2,4>triazepine-5,8-dione

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