1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE O-PROP-2-YNYL-OXIME

Base Information

Chemical Name:1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE O-PROP-2-YNYL-OXIME
CAS No.:314238-36-3
Molecular Formula:C₁₃H₂₁NO₂
Molecular Weight:223.315
Hs Code.:
Mol file:314238-36-3.mol

Synonyms:Bicyclo[2.2.1]heptan-2-one,1,7,7-trimethyl-, O-(oxiranylmethyl)oxime, (1R,4R)- (9CI)

Suppliers and Price of 1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE O-PROP-2-YNYL-OXIME

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE-O-PROP-2-YNYL-OXIME 95.00%
5MG
$ 496.16

Total 6 raw suppliers

Chemical Property of 1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE O-PROP-2-YNYL-OXIME

Chemical Property:

Boiling Point:258.4°Cat760mmHg
Flash Point:91.8°C
PSA：21.59000
Density:1g/cm³
LogP:2.83840

Purity/Quality:

98% ^*data from raw suppliers

1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE-O-PROP-2-YNYL-OXIME 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE O-PROP-2-YNYL-OXIME

There total 3 articles about 1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPTAN-2-ONE O-PROP-2-YNYL-OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 37850-13-8
(1R,E)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one oxime

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 314238-36-3
(1R,4R)-1,7,7-Trimethyl-bicyclo[2.2.1]heptan-2-one O-oxiranylmethyl-oxime

Guidance literature:: (1R,E)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one oxime; With sodium hydride; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

epichlorohydrin; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/S0014-827X(00)00065-3

Reference yield:

: 37939-80-3
1,7,7-trimethyl-bicyclo[2.2.1]heptane-2-one-oxime

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 314238-36-3
C₁₃H₂₁NO₂

Guidance literature:: 1,7,7-trimethyl-bicyclo[2.2.1]heptane-2-one-oxime; With methanol; sodium methylate; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

epichlorohydrin; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1080/14756366.2020.1838501