2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide

Base Information

• Chemical Name: 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide
• CAS No.: 1535-95-1
• Molecular Formula: C₁₂H₂F₈S₂
• Molecular Weight: 362.267
• Mol file: 1535-95-1.mol

Synonyms:2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide

Chemical Property of 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

BIS(2,3,5,6-TETRAFLUOROPHENYL)DISULFIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide

There total 3 articles about 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,3,5,6-tetrafluorothiophenol (769-40-4) → 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide (1535-95-1)

Guidance literature:

With bromine; acetic acid; at 20 ℃; for 24h; Sealed tube;

DOI:10.1134/S1070428021120046

Reference yield:

1-(2,3,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene → 2,3,5,6-tetrafluoroaniline (700-17-4) + 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide (1535-95-1) + 4,5,7-Trifluoro-2,1,3-benzothiadiazole (132844-31-6,530102-90-0)

Guidance literature:

With cesium fluoride; In acetonitrile; for 0.5h; Heating;

DOI:10.1002/ejic.200390016

Reference yield:

→ 2,2',3,3',5,5',6,6'-octafluorodiphenyl disulfide (1535-95-1)

Guidance literature:

ether. 2,3,5,6-Tetrafluor-phenylmagnesiumbromid, ether. S2Cl2, -30grad;

upstream raw materials:

2,3,5,6-tetrafluorothiophenol

Downstream raw materials:

[Mo(CO)3(SC₆F₄H)(C₅H₅)]

[MoTl(SC₆F₄H)4(C₅H₅)]