3-amino-2-phenyl-5-methoxy-1-indenone

Base Information

Chemical Name:3-amino-2-phenyl-5-methoxy-1-indenone
CAS No.:199987-33-2
Molecular Formula:C₁₆H₁₃NO₂
Molecular Weight:251.285
Hs Code.:

Synonyms:3-amino-2-phenyl-5-methoxy-1-indenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-2-phenyl-5-methoxy-1-indenone

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Technology Process of 3-amino-2-phenyl-5-methoxy-1-indenone

There total 6 articles about 3-amino-2-phenyl-5-methoxy-1-indenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 5415-11-2
3-(4-methoxyphenyl)-3-oxo-2-phenylpropanenitrile

: 199987-33-2
3-amino-2-phenyl-5-methoxy-1-indenone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -10 - 20 ℃;
DOI:10.1021/jo991968k

Reference yield: 15.0%

: 94-30-4
ethyl 4-methoxybenzoate

: 140-29-4
phenylacetonitrile

: 199987-33-2
3-amino-2-phenyl-5-methoxy-1-indenone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -10 - 20 ℃;
DOI:10.1016/S0040-4039(97)10181-2

Reference yield:

: 121-98-2
methyl 4-methoxybenzoate

: 199987-33-2
3-amino-2-phenyl-5-methoxy-1-indenone

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaH / tetrahydrofuran / Heating

2: 75 percent / LDA / tetrahydrofuran / -10 - 20 °C

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; 1: Condensation / 2: Cyclization;
DOI:10.1021/jo991968k